Product Notes
- 8661205 reads
1. E. I. du Pont de Nemours and Company technical product, m.p. 111–112°, was used.
2. The time required for the addition varies from 1.5 to 2 hours.
3. There must be an excess of sodium carbonate to prevent the troublesome frothing caused by the liberation of carbon dioxide near the end of the coupling reaction.
4. The addition must be regulated so as to prevent the formation of large chunks of sodium carbonate decahydrate.
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